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The synthesis of boron nitride by nitridation with boron anhydride (B4O3) is one of the important methods for industrial production of boron nitride. Due to the low melting point of boron anhydride (glass state is 294°C, crystalline state is 450-600°C), it becomes a high-viscosity melt at the nitriding temperature, which hinders the flow of ammonia and makes the reaction slow and extremely incompl...
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This is a method of synthesizing boron nitride by reacting borax and ammonium chloride as the main raw materials in an ammonia atmosphere. The two raw materials should be dehydrated and recrystallized separately before participating in the reaction. Borax is best dehydrated in a vacuum at 200~400°C. The recrystallization of ammonium chloride is to dissolve it into a saturated solution, filter to r...
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Transmission Electron Microscope (TEM) Transmission electron microscopy uses an electron beam that penetrates a sample to image, which requires the sample being observed to be "transparent" to the incident electron beam. Transmission electron microscopy is widely used in materials science and biology. Since electrons are easily scattered or absorbed by objects, the penetration is low, and the dens...
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Fisher's method is a relatively simple particle size measurement method, which is based on measuring the speed of air passing through the powder accumulation, and then obtaining the average particle size of the powder according to the Kozeny-Carman formula. However, the Fisher method is a relative measurement method, which cannot accurately determine the true particle size of the powder, and is on...
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Characterization and testing technology is the fundamental way to scientifically identify nanomaterials, understand their diverse structures, and evaluate their special properties. The main purpose of characterization of nanomaterials is to determine some physical and chemical properties of nanomaterials, such as morphology, size, particle size, chemical composition, crystal structure, band gap an...
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Characterization and testing technology is the fundamental way to scientifically identify nanomaterials, understand their diverse structures, and evaluate their special properties. The main purpose of characterization of nanomaterials is to determine some physical and chemical properties of nanomaterials, such as morphology, size, particle size, chemical composition, crystal structure, band gap an...
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The specific surface area is the surface area (㎡/g) of the substance per unit mass. It is one of the most important physical properties of ultra-fine powder materials, especially nano-powder materials. It is used to evaluate their activity, adsorption, catalysis and other properties. important physical properties. Therefore, in the research, manufacture and application of various ultrafine powder ...
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Manganese dioxide, also known as "manganese peroxide", "black manganese oxide", is a black orthorhombic crystal or brown-black powder, and there are many variants. Insoluble in water, nitric acid, cold sulfuric acid and acetic acid, soluble in cold and concentrated hydrochloric acid to generate unstable light brown-green MnCl4, which is heated and reacted with concentrated hydrochloric acid to rel...
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Supercapacitor is a new type of energy storage element, which is widely used in starting power supply, pulse power supply, military, mobile communication device, computer and electric vehicle due to its advantages of large capacity, fast charging and discharging of large current, and long cycle life. and other research fields. According to the different energy storage mechanisms, supercapacitors c...
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In order to obtain the correct data of the primary particle size, it is often necessary to open the agglomerated particles in the particle size test to form a particle monomer and keep it uniformly dispersed in the medium. This operation is called "dispersion". The requirement of the laser particle size analyzer for the dispersion system is "dispersion without segregation". Dispersion techniques a...
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