In transmission electron microscopy (TEM) analysis, the primary and crucial step in obtaining a high-quality image that can be interpreted reasonably is sample preparation. Inappropriate sample thickness, poor conductivity, or damage introduced during sample preparation can directly lead to abnormal electron beam penetration, image distortion, and even sample scrapping. TEM sample requirements ① T...
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What are nanoparticles? Nanoparticles (NPs) are typically defined as granular materials with at least one dimension at the nanoscale (1-100 nm) in three-dimensional space. From the dimensions of structure and morphology, nanoparticles can be classified into zero dimensional nanomaterials (0D nanomaterials), corresponding to one-dimensional (1D) and two-dimensional (2D) nanomaterials. 0D nanopartic...
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1.Characterization of particle size and distribution Dynamic Light Scattering (DLS): DLS is one of the most commonly used techniques for measuring the particle size and distribution of nanoparticles in suspensions. It calculates the hydrodynamic diameter of particles by measuring the time-dependent light scattering intensity fluctuations caused by Brownian motion of particles. DLS can also provide...
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XRD is an important means of characterizing phases. Strictly speaking, it can determine the existence of a certain phase, but cannot determine the absence of a certain phase, making it easier to distinguish between truth and falsehood. So, what is its detection limit? Firstly, we must emphasize that XRD analysis of elemental content is very inaccurate. If we have to say what the detection limit is...
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With the increasing demand for high thermal conductivity materials, filled thermal conductive polymer composites have good application prospects. The performance of thermal conductive composite materials largely depends on the selection of thermal conductive fillers. Aluminum oxide (Al2O3)is a common ceramic filler with high hardness and good thermal conductivity, and is a commonly used choice to ...
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Powder surface modification changes the surface state of particles through physical or chemical means, with the core being to break the agglomeration force between particles. When the particle size of the powder decreases to the micrometer or nanometer level, the surface energy sharply increases, and van der Waals forces, hydrogen bonds, and other gravitational forces cause the particles to sponta...
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